GCMS calibration table for TCLP analysis, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\DEC0 6 01 \LBA D [ (A Vial: 10 Acq On 6 Dec 2001 6:23 pm 653 %20bl70 Operator: GALOS Sanpl e Mise gc/ms unknown 11/7 400-61 Inst Multiplr: : GC/MS Ins 1.00 MS Integration Params: RTEINT.P 9016 Quant Time: Dec 19 13:07 2001 20

Quant Method : (2753o(uant Results File:

C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) NP112701.RES

Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.89 152 824674 20.00 ng/uL -0.05 19) Naphthalene-d8 15.50 136 3071416 20.00 ng/uL -0.05 31) Acenaphthene-diO 20.78 164 1396658 20.00 ng/uL -0.05 49) Phenanthrene-diO 25.18 188 1942752 20.00 ng/uL -0.06 59) Chrysene-dl2 33.18 240 1229507 20.00 ng/uL -0.06 68) Perylene-d12 37.27 264 756315 20.00 ng/uL -0.06

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 • 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.89 132 367 0.01 ng/uL 0.47 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 12.30 152 283 0.01 ng/uL -0.16 Spiked Amount 50.000 Range 26 73 Recovery = 0.02%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.92 172 880 0.01 ng/uL 0.09 Spiked Amount 50.000 Range 42 78 Recovery = 0.02%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2’-oxybis(1-Chloropropan 12.90 45 674 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration LBA.D NP112701.M Wed Dec 19 13:08:11 2001 Page 1

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