NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data Pile : C:\HPCHEM\1\DATA\DEC0701\26537.D Vial: 4
Acq On : 7 Dec 2001 8:51 pm Operator: GALOS
Sample : gc/ms unknown 11/6 Inst : GC/MS Ins
Mise Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Dec 10 9:26 2001 Quant Results File: NP112701.RES
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator)
Title : 208 625/TCLP calibration table
Last Update : Wed Nov 28 15:33:44 2001
Response via : Initial Calibration
DataAcq Meth : NP112701
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.88 152 866343 20.00 ng/uL -0.06
19) Naphthalene-d8 15.49 136 3292985 20.00 ng/uL -0.06
31) Acenaphthene-dl0 20.76 164 1499619 20.00 ng/uL -0.06
49) Phenanthrene-diO 25.17 188 2147738 20.00 ng/uL -0.07
59) Chrysene-dl2 33.18 240 1401662 20.00 ng/uL -0.07
68) Perylene-dl2 37.27 264 938390 20.00 ng/uL -0.07
System Monitoring Compounds
4) 2 -Fluorophenol 0.00 112 0 0.00 ng/uL
Spiked Amount 75.000 Range 18 42 Recovery = 0.00%#
5) Phenol-d5 0.00 99 0 0.00 ng/uL
Spiked Amount 75.000 Range 19 32 Recovery = 0.00%#
6) 2-Chlorophenol-d4 0.00 132 0 0.00 ng/uL
Spiked Amount 75.000 Range 34 84 Recovery = 0.00%#
7) 1,2-Dichlorobenzene-d4 12.14 152 656 0.02 ng/uL -0.32
Spiked Amount 50.000 Range 26 73 Recovery = 0.04%#
20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL
Spiked Amount 50.000 Range 55 98 Recovery = 0.00%#
32) 2-Fluorobiphenyl 18.92 172 1386 0.01 ng/uL 0.09
Spiked Amount 50.000 Range 42 78 Recovery = 0.02%#
33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL
Spiked Amount 75.000 Range 45 96 Recovery = 0.00%#
62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL
Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#
Target Compounds Qvalue
2) Pyridine 0.00 79 0 N.D.
3) N-nitrosodimethylamine 0.00 74 0 N.D.
8) Phenol 0.00 94 0 N.D.
9) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
10) 2-Chlorophenol 0.00 128 0 N.D.
11) 1,3-Dichlorobenzene 0.00 146 0 N.D.
12) 1,4-Dichlorobenzene 0.00 146 0 N.D.
13) 1,2-Dichlorobenzene 0.00 146 0 N.D.
14) 2-Methylphenol 0.00 108 0 N.D.
15) 2,2' -oxybis (1-Chloropropan 12.89 45 3017 N.D.
16) 3&4-Methylphenol 0.00 108 0 N.D.
(#) = qualifier out of range (m) = manual integration
26537.D NP112701.M Mon Dec 10 10:06:36 2001 Page 1
NYC-WTC_000031849
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