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GCMS analysis sample AD26537, non-target compounds, Dec 2001

Machine-extracted title · confidence 95%

Mass spectrometry analysis of sample AD26537 found no non-target compounds present, Dec 16, 2001.

NYC-WTC_000031847–000031868

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data Pile : C:\HPCHEM\1\DATA\DEC0701\26537.D Vial: 4 Acq On : 7 Dec 2001 8:51 pm Operator: GALOS Sample : gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 10 9:26 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.88 152 866343 20.00 ng/uL -0.06 19) Naphthalene-d8 15.49 136 3292985 20.00 ng/uL -0.06 31) Acenaphthene-dl0 20.76 164 1499619 20.00 ng/uL -0.06 49) Phenanthrene-diO 25.17 188 2147738 20.00 ng/uL -0.07 59) Chrysene-dl2 33.18 240 1401662 20.00 ng/uL -0.07 68) Perylene-dl2 37.27 264 938390 20.00 ng/uL -0.07

System Monitoring Compounds 4) 2 -Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ng/uL Spiked Amount 75.000 Range 34 84 Recovery = 0.00%# 7) 1,2-Dichlorobenzene-d4 12.14 152 656 0.02 ng/uL -0.32 Spiked Amount 50.000 Range 26 73 Recovery = 0.04%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.92 172 1386 0.01 ng/uL 0.09 Spiked Amount 50.000 Range 42 78 Recovery = 0.02%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%# Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2' -oxybis (1-Chloropropan 12.89 45 3017 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration 26537.D NP112701.M Mon Dec 10 10:06:36 2001 Page 1

NYC-WTC_000031849

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NYC-WTC_000031849Source: NYC Law Department, mirrored locally

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