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GCMS comments for sample AD26476 showing no non-target compounds

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Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26476 revealed no non-target compounds.

NYC-WTC_000031707–000031728

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC0701\26476.D . Vial: 6 Acq On 7 Dec 2001 10:40 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise ' Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 10 9:26 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.87 152 1154319 20.00 ng/uL -0.06 19) Naphthalene-d8 15.49 136 4383066 20.00 ng/uL -0.06 31) Acenaphthene-diO 20.77 164 1973804 20.00 ng/uL -0.05 49) Phenanthrene-diO 25.18 188 2782015 20.00 ng/uL -0.06 59) Chrysene-dl2 33.18 240 1632262 20.00 ng/uL -0.07 68) Perylene-dl2 37.26 264 1078483 20.00 ng/uL -0.07

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000. Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.88 132 718 0.01 ng/uL 0.46 Spiked Amount 75.000 Range 34 84 Recovery 0.01%# 7) 1,2-Dichlorobenzene-d4 12.26 152 297 0.01 ng/uL -0.20 Spiked Amount 50.000 Range 26 73 Recovery = 0.02%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.92 172 2166 0.02 ng/uL 0.08 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 12.87 45 1388 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration 26476.D NP112701.M Mon Dec 10 10:07:48 2001 Page 1

NYC-WTC_000031709

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NYC-WTC_000031709Source: NYC Law Department, mirrored locally

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