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GCMS analysis report for sample AD26477, Dec 2001

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DEP lab report dated December 21, 2001, documenting GCMS analysis of sample AD26477 with specific result and MDL values.

NYC-WTC_000031729–000031738

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C : \HPCHEM\ 1 \DATA\DEC2 10126477.D Vial: 54 Acq On : 21 Dec 2001 3:13 pm Operator: 209 GALOS Sample : gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.599 274 278 291 rBV 286258 867255 14.46% 2.840% 2 11.363) 684 688 693 rBV 29752 79435 1.32% 0.260% 3 11.437/ 693 696 703 rW 27701 75452 1.26% 0.247% 4 11.675 717 722 747 rBV 1440051 4483272 74.74% 14.682% 5 15.274 1109 1114 1135 rBV 2301933 5516756 91.97% 18.067%

6 20.553 1683 1689 1712 rBV 2651350 5998144 100.00% 19.643% 7 24.978 2164 2171 2184 rBV2 2178334 5437132 90.65% 17.806% 8 26.997 2385 2391 2399 rBV 43818 109959 1.83% 0.360% 9 30.054 2719 2724 2737 rBV 362807 759968 12.67% 2.489% 10 33.010 3040 3046 3067 rBV2 1610046 4066546 67.80% 13.318%'

11 37.105 3484 3492 3518 rBV 1018274 3141123 52.37% 10.287%

Sum of corrected areas: 30535042

26477.D GCMS1126.M Fri Dec 21 16:16:30 2001

NYC-WTC_000031734

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NYC-WTC_000031734Source: NYC Law Department, mirrored locally

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