GCMS analysis results for sample AD26319, Dec 2001

NYC 9/11 Public Portal Document

Library Search Comp: . Report Data File C:\HPCHEM\1\DATA\DEC050 3 .19.D Vial: 7 Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params.- LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\ . 7 01.M (RTE Integrator) Title 208 625/TCLP calibrer table Library C ; \DATABASE\NBS75K . !• ************************************* • < *************************** Peak Number 14 1-Monolinoleoylglycer i imet Concentration Rank 12

R.T. EstCon Area ‘6 tive to I STD R.T. 35.70 0.67 ng/uL 121617 F Y -dl2 37.25

Hit# of 5 Tentative ID MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethyls' 1 • C2715404Si2 054284-45-6 33 2 3-Trimethylsilyloxystearic acid, t 1 1 “24H5203Si2 000000-00-0 17 3 Pentanoic acid, 2-[(trimethylsilyl . 2 2 C11H2603Si2 . 055887-46-2 12 4 1H- Indole, 7-methoxy-__________ 1 ' C9H9110 003189-22-8 9 Abundance Scan 3365 (35.701 min): 26319. D (-1 m/z 73100 100.00% 73 | 147 | 5000 221 281 L-PAAA5 -PI ,, T T 35' 35.40 35/ " 35.80 36.00 191 _। - । m/z 14 7 . ' 0 57.77% I —vr IIl ——————— "T W n/z-> 50 100 150 200 250 300___ 350 50 Abundance 158871: 1-Monolinoleoylglycerol trimethylsi’ ‘ 73

'A । 207 5000 i 147 11 1 1 ■I • ' ■ 1 I 35.40 35.60 35.80 36.00 ! 34 ■ 103 | m/z 221.0 5 32.11% 281 n0 i 482 1 m/z-> 50 100 150 200 250 300 350 4 450 | Abundance #55734: 3-Trimethylsilyloxystearic acid, trimet!" 73 ■ ■ i 1 r • _________ TE/nn/ 35.40 35.00 35.80 36.00 50001 147 233 m/ z 2 81.10 22.98% I 313 189 | 339 i T-r--r-r- — "11 T-05*1m. . I * — ——— n/z->_____ Abundance 50 100 150 200 250 300 350 #733156: Pentanoic acid, 2-[(trimethylsily l)oxy)-. .IF 40—— - 1 73 35.40 35.63 35.80 36.00 131 m/z 20 6.95 18.38%

5000- ... M j 46 95 ; I 205 247 ■ ■ i ■ ■ ■ ■ i ■ 1 1 1 i m/z-> 50 100 150 200 250 300 350 450 35.40 35.60 35.50 36.00

26319.D NP112701.M Wed Dec 05 1. :0 33 2001 Page 14

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