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GCMS analysis results for sample AD26319, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26319 with unidentified compounds detected.

NYC-WTC_000031297–000031318

Folder label: “GCMS X 11/3/01 A 12/1/01

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Scanned page image, NYC-WTC_000031316
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NYC 9/11 Public Portal Document

Library Search Compel Report Data File C:\HPCHEM\1\DATA\DEC050., 19 .D Vial: 7 Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C : \HPCHEM\1\METHODS\:"' ”701.M (RTE Integrator) Title 2 08 62 5/TCLP calibrat . table Library C:\DATABASE\NBS75K.L ************************************* : * *************************** Peak Number 13 3-Isopropoxy-1,1,1,7, ’ ram Concentration Rank 10

R.T. EstConc Area uive to ISTD R .T.

34.51 0.82 ng/uL 199475 C. ne-dl2 33.17

Hit# of 5 Tentative ID MolForm CAS# Qual 1 3 - Isopropoxy-1,1,1,7,7,7-hexamethy • C18H5207Si7 071579-69-6 33 2 Ethanedioic acid, bis (trimethylsil CBH1804Si2 018294-04-7 32 3 1,1,1,5, 7,7, 7 -Heptamethyl - 3 , 3 -bis ( . . C131I40O5Si6 038147-00-1 25 4 2-Ethyl- -trimethylsilyloxy (crime: : C12112803Si2 000000-00-0 23 Abundance i Scan 3235 (34.509 min): 26319.D () m/ 73.05 100.00% 73 | 1 1 5000- 147 221 281 ............. 355 34.20 34.40 34.60 34.80 327 i 4* n . . . । । । m/z 147.10 46.59% m/z->____ 50 100 150 200 250 300 350 400 ′( 5.) 550 i Abundance #60503: 3-Isopropexy-1 ,1,1,7,7,7-hexamethyl-3. 73 ii ■’ V : \ 5000 - S...... ....... 147 34.20 34.40 34.60 34.80 m/z 2 21.05 28.16% 221 21 327 417 519 561 1 ■ i m/z->__ 50 100 150 200 250 300 350 400 5 70 550 Abundance #71005: Ethanedioic acid, bis(trimeti ylsily!) er 73 / 0 pr-rrT-f 147 3.1.20 34.40 34.60 34.80 5000- ; m/2 281.00 16.79% /, J 45 jl |L TT l 117 190 219 - — ' P IIPTII 1 m/z->______ 50 Abundance 73 100 150 200 250 300 350 400 #56714:1,1,1,5,7,7,7-Heplamethyl-3,3-bis(trim-: • :2 550 IAA ! 34.20 34.40 34.60 34.80 ! m/ z 355.05 15.64% 147 5000 267 1 | 355 45 207 | 1 07 . 1 I I I -Hr 1 Te I 1 1. "T T T m/z-> 50 100 150 200 250 300 350 400 J0 550 ! 34.20 34.40 34.60 34.80

26319.D NP112701.M Wed Dec 05 1. 2 ; 2001 Page 13

NYC-WTC_000031316

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NYC-WTC_000031316Source: NYC Law Department, mirrored locally

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