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GCMS analysis results for sample AD26319, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26319 with unidentified compounds detected.

NYC-WTC_000031297–000031318

Folder label: “GCMS X 11/3/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compou:. ’ Report Data File C:\HPCHEM\1\DATA\DECO5O1\: '319.D vial: 7 . Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C:\HPCHEM\1\METHODS\NP .2701.M (RTE Integrator) Title 208 625/TCLP calibrati : table Library C:\DATABASE\NBS75K.L ********* ****************************** ■ ****************************

Peak Number 5 Cyclohexasiloxane, dodo methy Concentration Rank 2 R.T. EstConc Area ative to ISTD R.T. 17.65 5.62 ng/uL 2129460 Nan . .halene-d8 15.48

Hit# Of 5 Tentati ID ‘W MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 4 C12H3606Si6 000540-97-6 72 2 2H-1,4 -Benzodiazepin- 2 - one, 7-chlor 2 C18H19ClN2OSi 055299-24-6 22 3 Silane, 1,2,3-benzenetriyltris(oxy . 2 C15H30O3Si3 017864-23-2 10 4 Silane, 1,2,3-benzenetriyltris (oxy ■ 2 C15H30O3Si3 017864-23-2 10 Abundance Scan 1396 (17.645 min): 26319.0 (-) m/ z 73.05 100.00% 73

5000 3-. 1 147 429 17.40 17.60 17.80 18.00 45 117 i 179 207225 251 23! 311 [ : 397 | TT "Tmmgtmptemmn —"OTmm3n. • Tag m/z 340.95 30.47% n/z-> 40 60 80 100120140 160 180 200 220 240 260 280 300 320 3d " ) 380 400 420 Abundance #56/11: Cyclohexasiloxane, dodecamethyi- 73 3'

5000 429 1I 17.40 17.60 17.80 18.00 m/z 429.10 13.65% 117 147 | 2°7 267 311 I I “i1"' • TIrm. ............................................ "I""i “ni""I'11' •T. TTEUTmu m/z->___ 40 60 80 100120140 160 180 200 220 240 260 280 300 320 3- ' .1380400420 Abundance #4833/: 2H-1,4-Benzodiazepin-2-one, /-chloro-1,3-c"i --5- 73 3-;: T 1 ' ' I 17.40 17.60 17.80 18.00 5000 m/z 147.00 13.43% 45

—11 146 227 269 315. m/z-> 40 60 80 100120 140 160 130 200 220 240 260 280 300320 2- : ) 380 400 420 Abundance #73587: Silane, [1,2,3-benzenetriyltris(oxy))tris[lri;: 70 239 17.40 17.60 17.80 18.00 m/z 324.95 10.42%

5000

45 133 |— .- 211 l \ l,,nl T I' T r" " i ‘' i' i" " r ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 3- ' } 380 400 420 17.40 17.60 17.80 18.00

’ 26319.D NP112701 .M Wed Dec 05 15 :32 2001 Page 5

NYC-WTC_000031308

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NYC-WTC_000031308Source: NYC Law Department, mirrored locally

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