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Document / 22 pages

GCMS analysis results for sample AD26319, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26319 with unidentified compounds detected.

NYC-WTC_000031297–000031318

Folder label: “GCMS X 11/3/01 A 12/1/01

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Scanned page image, NYC-WTC_000031307
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NYC 9/11 Public Portal Document

Library Search Compou?! 1 Report Data File C : \HPCHEM\1\DATA\DEC0501\2 5319 .D vial: 7 Acq On 5 Dec 2001. 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\Np" .2701.M (RTE Integrator) Title 208 625/TCLP calibrati: . table Library C:\DATABASE\NBS75K.L ******************************* * * ****** r ************************** * **

Peak Number 4 Cyclopentasiloxane, decrethyl Concentration Rank 5

R .T. EstConc Area Re ative to ISTD R.T. 14.50 2.17 ng/uL 822946 Nap!' '.halene-d8 15.48 Hit# of 5 Tentative ID IW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- • '0 C10H3005Si5 000541-02-6 50 2 Benzoic acid 2, 5-bis(trimethyIsilo : 0 C16H30O4Si3 003618-20-0 47 3 3,4 -Dihydroxybenzyl alcohol, tris (tr 2 6 C16H3203Si3 068595-79-9 38 4 N- (Trifluoroacetyl) -0,0' , O' ‘-tris (t 1 C19H34F3NO4Si3 000000-00-0 37 Abundance " D (-) Scan 1053 (14,500 min): 26319. " m/z 73.05 100.00% 73

5000- 267 355 "II 45 14.20 14.40 14.60 14.80 , 108 133 154 177193 223 251 1 323339 1 ' ■ ।1 ■ "TPITTe —Ir “TTTTTTTTNTTTTTT)T "TTTITT - m/z 267.00 28.54% m/z-> 40 GO 80 100 120 140 160 180 200 220 240 260 280 3' 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 | ■ 1 ■ i T 1420 14 40 14.60 14.80 m/z 355.05 24.21% 251 । 191207 323339 ] TI‘ i1 ■ ■ ■ I ■ T’T TTTITTTr T — T 'l l ■■■' l m/z->_____ 40 60 80 100 120 140 160 180 200 220 240 260 280 3 320 340 360 Abundance #73978: Benzoic acid, 2,5-bis(trimethyisiloxy)-, trime. Is 73 355 ) 1 * i < ■ ■ ■ । ■ ’ TI 14.20 14.40 14.60 14.80 5000 m/z 356.05 8.28% 45 fl 147 179 207223 267282 | 370 ’ r TT ! "TTil ’• —9 -I—nT- -0 * 11111* p " ' i • * TIT "‘"I m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 3 320 340 360 Abundance #49868: 3.4-Dihydroxybenzyl alcohol, tris(trimethyls. , T । ■ ■ ■ 1 । 1 ■ l ■ • ■ * l !i 73 14.20 1440 1460 14.80 m/z 74.05 8.18% 267 5000 179 356 45 147 L - 299 237 — ;2 341 }... r* * ■1TT 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 3:. 320 340 360 14.20 14.40 14.60 14.80

26319.D NP112701.M Vied Dec 05 15 : : 32 2001 Page 4

NYC-WTC_000031307

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NYC-WTC_000031307Source: NYC Law Department, mirrored locally

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