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← Document results/DEP Box 20/525 X 10/19/01 10/22/01 AN 11/3 - 11/5/01
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Method detection limit verification for sample AD24488, Nov 2001

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Laboratory report verifying method detection limits for pesticides in sample AD24488 analyzed in November 2001.

NYC-WTC_000028798–000028802

Folder label: “525 X 10/19/01 10/22/01 AN 11/3 - 11/5/01

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"O l C O O O O Integration Report Quanfile: MDLB1103 Quan Entries: 28 CT O' N co Comment: BOHLK: METHOD 525; INST 204; 11/03/01; MDL U O co Sorted via: Entry Number 1 — O 9 0 0 No Name of Compound R Time Scani Node Peak Area Pk Height 0 C 3 CD S 3 chrysene d-12(IS) 22:45 1365 Auto 1,906,816 685,453 4 p-terphenyl d-14(IS) 20:54 1254 Auto 2,869,729 1,733,480 5 acenaphthene d-10(SURR 12:21 741 Auto 1,752,488 1,167,732 6 phenanthrene d-10(SURR 17:00 1020 Auto 2,649,067 1,132,819 7 chrysene d-12 (SURE) 22:45 1365 Auto 1,906,816 685,453 8 1,3-d imethy1-2-n itrobe 8:01 481 Auto 1,106,275 612,692 9 triphenyl phosphate (S 22:10 1330 Auto 1,414,024 514,090 10 perylene d-12 CSURR) 27:07 1627 Auto 1,275,319 249,011 11 hexachlorocycIopentadi 10:12 612 Auto 12,497 7,536 12 hexach lorobenzene 15:25 925 Auto 51,204 19,222 13 simazine 16:10 970 Auto 13,677 4,344 14 atrazine 16:21 981 Auto 17,514 5,586 15 alachlor 18:27 1107 Auto 43,948 25,223 16 bis(2-ethyIhexy DJadipa 22:03 1323 Auto 42,558 8,064 17 b is(2-ethyIhexyl phtha 23:03 1383 Auto 511,293 134,579 18 benzo(a)pyrene 26:53 1613 Auto 20,698 2,700 19 eptc 10:36 636 Auto 859,375 432,422 20 2,6-d in itrotoluene 11:59 719 Auto 224,302 93,942 21 2,4-d in itrotoluene 12:58 778 Auto 228,104 88,835 22 mol inate 13:86 786 Auto 331,594 207,094 23 terbac il 17:25 1045 Auto 262,652 97,532 24 acetochlor 18:16 1096 Auto 241,937 121,078 25 metribuzin 18:18 1098 Auto 30,770 12,088 26 metolachlor 19:12 1152 Auto 119,157 52,776 27 butachlor 28:26 1226 Auto 39,843 22,740 28 4,4% —dde 20:49 1249 Auto 179,543 116,341

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NYC-WTC_000028801Source: NYC Law Department, mirrored locally

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