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Spiked sample analysis AD27009, Nov-Dec 2001

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DEP laboratory spiked sample analysis (SC1525) for sample AD27009 conducted on November 30, 2001.

NYC-WTC_000030535–000030551

Folder label: “525 11/13/01 - 11/30/01 12/6 12/17 12/20/01

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0 “0 I C o o o Integration Report Quanfile: MDLB1129 Quan Entr ies: 28 O o o C Comment: BOHLK: METHOD 525; INST 204; 11/29/01; MDL U O 0 CH Sorted via: Entry Number T — 0 CH O No Name of Compound R Time Scan# Node Peak Area Pk Height 0 0 C 3 CD 3 chrysene d-12(IS) 22:36 1356 Auto 1,537,055 716,906 D 4 p-terphenyl d-14(IS) 20:47 1247 Auto 4,136,444 2,614,788 5 acenaphthene d-10(SURR 12:13 733 Auto 1,101,091 568,750 6 phenanthrene d-10CSURR 16:49 1009 Auto 1,901,072 703,259 7 chrysene d-12 (SURR) 22:36 1356 Auto 1,537,055 716,906 8 1,3-d imethy1-2-n itrobe 7:54 474 Auto 641,019 359,744 9 triphenyl phosphate (S 22:01 1321 Auto 844,438 391,182 10 perylene d-12 CSURR) 26:49 1609 Auto 1,151,886 223,976 11 hexachlorocyclopentad i 10:04 604 Auto 3,121 2,266 12 hexachlorobenzene 15:14 914 Auto 29,049 12,136 13 simazine 16:01 961 Auto 5,890 1,648 14 atrazine 16:10 970 Auto 13,208 3,679 15 alachlor 18:19 1099 Auto 32,844 19,169 16 bis (2-ethyIhexy Dad ipa 21:54 1314 Auto 54,672 15,984 17 b is(2-ethyIhexyl phtha 22:53 1373 Auto 342,182 126,962 18 benzo(a)pyrene 26:36 1596 Auto 63,000 7,942 19 eptc 10:29 629 Auto 469,038 258,272 20 2,6-d in itrotoluene 11:52 712 Auto 124,691 38,136 21 2,4-d in itrotoluene 12:52 772 Auto 120,504 18,664 22 molinate 12:58 778 Auto 191,001 114,136 23 terbac i1 17:16 1036 Auto 159,051 36,215 24 acetochlor 18:07 1087 Auto 190,621 115,154 25 metribuzin 18:10 1090 Auto 17,752 7,107 26 metolachlor 19:05 1145 Auto 84,760 34,160 27 butachlor 20:19 1219 Auto 33,396 19,550 28 4,4'-dde 20:42 1242 Auto 116,350 76,455

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NYC-WTC_000030545Source: NYC Law Department, mirrored locally

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