Quality control analyses log, Oct 2001

2 Z K K o o co 3 _s

"0 O C 1 CT O O O Mass List File: E:\DFTA1025 Date: Oct-25-1991 18:36:30 5' O N co Comment: BOHLKi METHOD 525; INST 204; 10/25/01; DFTPP/ENDRIN "0 o N Scan No: 1111 Retention Time: 18:31 RIC: 6756526 Mass Range: 49 - 444 — 9 C # Peaks: 167 Mass of Base Peak: 442 Int: 1272569 Threshold: 0 % U o o C Mass Intensity % Base Mass Intensity % Base Mass Intensity % Base 3 CD — 49 22,569 1.77 85 4,861 0.38 128 17,013 1.34 50 130,208 10.23 86 10,069 0.79 129 93,750 7.37 / 51 397,569 31.24V 87 4,513 0.35 130 10,763 0.85 52 17,013 1.34 91 7,291 0.57 131 3,125 0.25 55 6,250 0.49 92 4,861 0.38 134 2,777 0.22 56 11,458 0.90 93 39,930 3.14 135 7,291 0.57 57 19,444 1.53 94 3,472 0.27 136 3,472 0.27 61 6,250 0.49 98 40,277 3.17 137 2,777 0.22 62 6,944 0.55 99 17,013 1.34 141 15,972 1.26 63 9,722 0.76 100 4,513 0.35 142 5,555 0.44 64 3,472 101 8,680 0.68 143 3,472 0.27 68 69 6,944 293,055 208.8 23.03 103 104 7,638 10,763 0.60 0.85 146 147 3,472 8,333 0.27 0.65 73 8,333 20 0.65 105 9,375 0.74 148 18,055 1.42 74 46,875 3.68 107 93,750 7.37 149 2,777 0.22 75 35,763 2.81 108 12,500 0.98 153 3,125 0.25 76 16,666 1.31 109 3,125 0.25 154 5,902 0.46 77 276,736 21.75 110 171,527 13.48 155 7,986 0.63 78 15,972 1.26 ill 18,402 1.45 156 11,111 0.87 79 36,111 2.84 117 121,180 9.52 157 4,513 0.35 80 18,055 1.42 118 9,375 0.74 160 3,472 0.27 81 21,875 1.72 122 6,597 0.52 161 6,944 0.55 82 4,861 0.38 123 11,111 0.87 162 2,777 0.22 83 5,208 0.41 125 3,472 0.27 165 7,638 0.60 84 5,555 0.44 127 203,125 15.96 166 3,819 0.30