GC/MS data fragment, May 28 2002

NYC 9/11 Public Portal Document LSC Area Percent Report: Data File : C:\MSDCHEM\1\DATA\051702\11416.D Vial: 25 Acq On : 18 May 2002 9:10 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.708 96 107 110 PV 5 3974 105343 0.29% 0.048% 2 3.731 110 111 112 W 3399 34011 0.09% 0.016% 3 3.749 112 114 116 W 3 3692 41224 0.11% 0.019% 4 4.231 193 196 199 W 4 2148 29206 0.08% 0.013% 5 5.024 327 331 337 PV 2 2996 61701 0.17% 0.028%

6 5.394 391 394 397 W 5 2074 28362 0.08% 0.013% 7 5.964 483 491 514 PV 628355 11335715 30.68% 5.219% 8 6.105 514 515 522 W 5 1960 31295 0.08% 0.014% 9 7.157 687 694 706 BV 9 1839 46242 0.13% 0.021% 10 7.733 788 792 801 W 3 5534 152867 0.41% 0.070%

11 7.791 801 802 808 W 4 2539 39332 0.11% 0.018% 12 9.930 1157 1166 1184 PV 1286903 24680939 66.80% 11.363% 13 10.065 1184 1189 1197 W 7 2386 55398 0.15% 0.026% 14 12.404 1583 1587 1594 W 3 2194 38727 0.10% 0.018% 15 13.426 1751 1761 1782 PV 1817518 33636015 91.04% 15.486%

16 13.579 1782 1787 1796 W 2 6139 117541 0.32% 0.054% 17 16.746 2321 2326 2331 PV 3 2410 35719 0.10% 0.016% 18 17.151 2386 2395 2401 W 4 6454 112954 0.31% 0.052% 19 17.657 2478 2481 2487 W 4 3051 44954 0.12% 0.021% 20 18.567 2617 2636 2662 PV 1955633 36947751 100.00% 17.011%

21 20.547 2961 2973 2989 PV 1199122 22863920 61.88% 10.526% 22 21.399 3110 3118 3123 W 2 8853 138991 0.38% 0.064% 23 22.574 3311 3318 3327 PV 3 10613 208951 0.57% 0.096% 24 22.950 3366 3382 3402 PV 2 1732026 35579385 96.30% 16.381% 25 23.109 3402 3409 3430 W 2 12710 392294 1.06% 0.181%

26 26.505 3981 3987 4005 W 2 1964 39262 0.11% 0.018% 27 30.806 4705 4719 4752 PV 2 1286850 28849441 78.08% 13.282% 28 31.012 4752 4754 4757 W 2 4102 50038 0.14% 0.023% 29 31.041 4757 4759 4773 W 3 2653 70739 0.19% 0.033% 30 31.376 4808 4816 4825 BV 4 4641 88072 0.24% 0.041%

31 34.702 5371 5382 5426 PV 878548 21293187 57.63% 9.803% 32 34.972 5426 5428 5441 W 6 2752 54909 0.15% 0.025%

Sum of corrected areas: 217204485

11416.D 050102.M Tue May 21 15:58:20 2002 Page 1

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