GC/MS analysis results for sample AE11416, May 28 2002

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Data File : C:\MSDCHEM\1\DATA\051702\11415.D Vial: 24 Acq On : 18 May 2002 8:21 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.667 94 100 103 PV 6 2025 38811 0.09% 0.016% 2 3.714 103 108 110 W 4 3128 58318 0.14% 0.025% 3 3.737 110 112 114 W 2 3262 35171 0.09% 0.015% 4 3.761 114 116 123 W 5 2978 83832 0.20% 0.036% 5 4.155 178 183 188 W 5 2585 57317 0.14% 0.024%

6 4.243 194 198 203 W 6 2699 50212 0.12% 0.021% 7 4.936 309 316 325 W 4 9629 170606 0.41% 0.072% 8 5.030 328 332 350 W 10 3931 124567 0.30% 0.053% 9 5.406 392 396 405 W 7 2594 68781 0.17% 0.029% 10 5.623 427 433 445 W 5 5744 153107 0.37% 0.065%

11 5.964 483 491 521 PV 588687 10695744 25.97% 4.536% 12 7.739 789 793 808 PV 4 5375 137932 0.33% 0.059% 13 9.936 1157 1167 1192 PV 1485079 28349443 68.82% 12.024% 14 12.404 1581 1587 1596 PV 1805 36116 0.09% 0.015% 15 13.426 1745 1761 1782 PV 2102605 38246026 92.85% 16.221%

16 13.579 1782 1787 1793 W 3 6685 118865 0.29% 0.050% 17 16.740 2318 2325 2339 PV 2 2757 48407 0.12% 0.021% 18 17.151 2390 2395 2400 W 2 5838 79473 0.19% 0.034% 19 17.662 2475 2482 2487 BV 3 2326 38655 0.09% 0.016% 20 18.567 2625 2636 2647 PV 2145829 41192300 100.00% 17.471%

21 18.644 2647 2649 2667 W 6 3170 84438 0.20% 0.036% 22 20.541 2960 2972 2991 W 1078140 20330048 49.35% 8.623% 23 21.393 3110 3117 3124 W 2 6798 112062 0.27% 0.048% 24 22.580 3308 3319 3330' BV 3 14749 253598 0.62% 0.108% 25 22.951 3361 3382 3402 PV 2 1920622 39490617 95.87% 16.749%

26 23.109 3402 3409 3422 W 14745 377457 0.92% 0.160% 27 30.806 4707 4719 4758 PV 2 1432284 32192519 78.15% 13.654% 28 31.047 4758 4760 4768 W 4 2825 80428 0.20% 0.034% 29 31.376 4811 4816 4828 PV 6 1947 42640 0.10% 0.018% 30 34.702 5361 5382 5420 PV 942263 22975716 55.78% 9.745%

31 34.937 5420 5422 5431 W 8 2378 55033 0.13% 0.023%

Sum of corrected areas: 235778241

11415.D 050102.M Tue May 21 15:57:40 2002 Page 1

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