GCMS analysis results for sample AE11409, May 22 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11384.D Vial: 11 Acq On : 17 May 2002 8:56 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 1,3-Dioxane-2-propanol , 2-m... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 7.74 0.24 ug/L 175832 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxane-2-propanol, 2-methyl- 160 C8H1603 036651-31-7 17 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0/9 3 2-Propanone, 1-(1-methylethoxy)- 116 C6H1202 042781-12-4 9 4 1-Pentanamine 87 C5H13N 000110-58/7 7 Abundance Scan 793 (7.739 min): 11384.D (-788) (-) m/z 43.10 100.00% 43

5000 WWWMWrww 87 - 1 1 ■ 1 ■ ■ | 1 ■ > ■ | r । | > । i i | 36 । 59 98.................................... ....1.1,Il —l TFT 1113 7.40 7.60 7.80 8.00 01 m/z 87.10 27.03% m/z-> Abundance 20 30 40 50 60 70 80 90 #5776:1,3-Dioxane-2-propanol, 2-methyl- 100 110 120 130 140 150 I 43 58

5000 ■ ■ i - ■ ■ ■ ।

84 7.40 7.60 7.80 8.00 m/z 41.10 16.56%

n/z-> 0- ■ ■ j ■ ■ ■ ■ i ■ ■ ■ ■ । । 20 30 40 L 544 d 111 'r111111I 50 60 70 80 101 i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ' ' 1 i j 90 100 110 120 130 140 150 145 ‘ i 1 ' 1 1 I 1 1 1 1 I 1 '

Abundance #4163: 3-Pyrrolidinol 43 ■ I ।,1 ■1 1 , , M i < 7.40 7.60 7.80 8.00 5000 m/z 59.10 15.20%

57 87 68 1 . n । । । > । । । । । । 01 ■ . । ' 1 । . . . 1 । । । ■ ■ 11 । । । । ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #4364: 2-Propanone, 1 -(1 -methylethoxy)- ■ > । ■ ■ ■ ■ i 43 7.40 7.60 7.80 8.00 m/ Z 98.10 13.89% 5000

27 58 73

/z-> O—TT .11,381 20 30 40 pl,. 50 60 70 | 83 80 90 101 100 110 120 115 130 140 150 7.40 7.60 1 1 1 1 1 1 I ' 1 1 1 I 7.80 8.00

11384.D 050102.M Tue May 21 11:56:14 2002 Page 5

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