GCMS analysis results for sample AE11382, May 22 2002

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Data File : C:\MSDCHEM\1\DATA\051702\11381.D Vial: 8 Acq On : 17 May 2002 6:29 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # ' min scan scan scan TY height area % max. total

1 3.120 3 7 23 BV 4 2999 84604 0.16% 0.026% 2 3.326 36 42 47 PV 2 8977 141787 0.26% 0.044% 3 3.379 47 51 56 W 6 3838 63134 0.12% 0.019% 4 3.608 83 90 97 PV 19723 310392 0.57% 0.096% 5 3.708 100 107 109 W 5 4436 92383 0.17% 0.028%

6 3.737 109 112 116 W 2 5756 102049 0.19% 0.031% 7 4.160 177 184 189 W 5 2908 61338 0.11% 0.019% 8 4.254 189 200 211 PV 9 2743 91021 0.17% 0.028% 9 5.030 323 332 338 PV 6 2569 49186 0.09% 0.015% 10 5.095 338 343 347 W 7 3800 69943 0.13% 0.022%

11 5.412 392 397 402 W 4 3050 69378 0.13% 0.021% 12 5.553 414 421 423 PV 6 2728 52206 0.10% 0.016% 13 5.576 423 425 427 W 2 2429 22786 0.04% 0.007% 14 5.653 434 438 447 W 6 2670 78821 0.14% 0.024% 15 5.976 485 493 528 W 951031 16994978 31.19% 5.242%

16 7.445 738 743 751 W 7 2601 49313 0.09% 0.015% 17 7.727 782 791 805 PV 2 12223 296939 0.55% 0.092% 18 8.814 972 976 988 W 6 3336 86050 0.16% 0.027% 19 9.302 1054 1059 1067 W 6 2679 65127 0.12% 0.020% 20 9.936 1156 1167 1198 PV 2008933 37390786 68.63% 11.533%

21 10.259 1212 1222 1226 PV 4 2105 25110 0.05% 0.008% 22 11.863 1491 1495 1506 W 6 2976 52184 0.10% 0.016% 23 12.040 1520 1525 1534 W 3115 53055 0.10% 0.016% 24 12.404 1576 1587 1595 PV 43676 672446 1.23% 0.207% 25 12.527 1604 1608 1617 PB 5 1616 24984 0.05% 0.008%

26 13.432 1745 1762 1781 PV 2658322 49845525 91.49% 15.374% 27 13.579 1781 1787 1798 W 2 8159 161460 0.30% 0.050% 28 15.700 2144 2148 2153 PV 2 2051 32327 0.06% 0.010% 29 16.746 2320 2326 2336 W 2 4425 86193 0.16% 0.027% 30 17.145 2382 2394 2402 PV 3 8840 149418 0.27% 0.046%

31 17.663 2473 2482 2487 PV 3 4295 69849 0.13% 0.022% 32 18.567 2613 2636 2648 PV 2699255 54482810 100.00% 16.805% 33 18.644 2648 2649 2658 W 6 3235 75028 0.14% 0.023% 34 18.961 2697 2703 2712 W 3 2070 39125 0.07% 0.012% 35 20.547 2958 2973 2988 PV 1451743 27823854 51.07% 8.582%

36 21.399 3108 3118 3128 W 4 12395 234141 0.43% 0.072% 37 22.580 3310 3319 3328 PV 2 22301 412092 0.76% 0.127%

11381.D 050102.M Tue May 21 14:25:18 2002 Page 1

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