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GCMS calibration data for sample AE11379, May 21, 2002

Machine-extracted title · confidence 95%

Calibration report for GCMS analysis of sample AE11379 performed on May 21, 2002, listing response factors for target analytes.

NYC-WTC_000025072–000025075

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document yudiiL J. LaL.Oll KEDOL L (V Kevlewed)

Data File C:\MSDCHEM\l\DATA\051702\CAL20.D Vial: 15 Acq On 18 May 2002 1:00 am Operator: Mclean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 21 12:01:35 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 19448241 23.51 ug/L 99 3 8) Pyrene 27.18 202 18704970 21.16 ug/L 97 39) Butylbenzylphthalate 29.52 149 8696967 22.07 ug/L # 94 40) Benzo(a)anthracene 30.79 228 13657122 19.40 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.38 149 11753523 22.07 ug/L 96 42) Chrysene 30.89 228 15353438 21.06 ug/L 98 44) Di-n-octylphthalate 33.24 149 16071726 20.14 ug/L 97 45) Benzo(b)fluoranthene 33.76 252 15483773 23.66 ug/L 97 46) Benzo(k)fluoranthene 33.83 252 17490666 21.27 ug/L 99 47) Benzo(a)pyrene 34.56 252 14924511 22.85 ug/L 99 48) Indeno(1,2,3-cd)pyrene 37.40 276 11792590 25.75 ug/L 100 49) Dibenz(a,h)anthracene 37.52 278 12453525 25.57 ug/L 98 50) Benzo(g,h,i)perylene 38.14 276 11528210m 22.54 ug/L

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL20.D 050102.M Tue May 21 12:02:10 2002 Page 2

NYC-WTC_000025074

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NYC-WTC_000025074Source: NYC Law Department, mirrored locally

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