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GCMS analysis results for sample AE11378, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE11378 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000025031–000025040

Folder label: “GCMS X 5/14/02 A 5/21/02

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Scanned page image, NYC-WTC_000025036
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C : \HPCHEM\ 1 \DATA\MAY2 10211377.D Vial: 26 Acq On : 22 May 2002 1:24 am Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.115 331 335 341 rBV 720569 1402218 40.62% 7.345% 2 9.920 528 532 540 rBV 13751 34896 1.01% 0.183% 3 12.137 769 774 792 rBV 1151465 2645781 76.64% 13.858% 4 15.775 1165 1171 1188 rBV 1720323 3452042 100.00% 18.082% 5 21.081 1743 1750 1771 rBV 1654757 3446838 99.85% 18.054%

6 23.216 1976 1983 1994 rBV 725621 1508904 43.71% 7.904% 7 25.516 2228 2234 2244 rBV2 1416504 3004163 87.03% 15.736% 8 27.496 2445 2450 2457 rBV 37261 71758 2.08% 0.376% 9 33.571 3107 3113 3136 rBV2 864629 1981013 57.39% 10.376% 10 37.786 3565 3573 3593 rBV2 530172 1543914 44.72% 8.087%

Sum of corrected areas: 19091527

11377.D GCMS0520.M Wed May 22 09:22:06 2002

NYC-WTC_000025036

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NYC-WTC_000025036Source: NYC Law Department, mirrored locally

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