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GCMS analysis results for sample AE11310, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE11310 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000025012–000025021

Folder label: “GCMS X 5/14/02 A 5/21/02

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Scanned page image, NYC-WTC_000025017
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\MAY2102\11309.D Vial: 23 Acq On : 21 May 2002 10:27 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.118 332 336 341 rBV 733804 1495955 42.73% 7.984% 2 9.914 528 532 538 rBV 15268 37220 1.06% 0.199% 3 12.141 769 775 797 rBV 1232060 2700558 77.13% 14.412% 4 15.779 1166 1172 1186 rW 1660358 3501347 100.00% 18.686% 5 21.076 1744 1750 1767 rBV 1653462 3454102 98.65% 18.434%

6 23.220 1975 1984 1997 rBV 801849 1606446 45.88% 8.573% 7 25.520 2228 2235 2245 rBV2 1419259 2951777 84.30% 15.753% 8 27.499 2446 2451 2459 rBV 34530 68481 1.96% 0.365% 9 33.575 3107 3114 3130 rBV 762375 1692386 48.34% 9.032% 10 37.781 3565 3573 3590 rBV2 409767 1229362 35.11% 6.561%

Sum of corrected areas: 18737634

11309.D GCMS0520.M Wed May 22 09:21:32 2002

NYC-WTC_000025017

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NYC-WTC_000025017Source: NYC Law Department, mirrored locally

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