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GCMS analysis results for sample AE10301, May 10, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10301 conducted on May 10, 2002, including surrogate recovery data.

NYC-WTC_000024927–000024934

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020509\10301.D Vial: 26 Acq On : 10 May 2002 11:20 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.152 512 523 549 rBV 586651 1143175 21.61% 4.026% 2 11.376 1399 1412 1436 rBV 1484835 3733630 70.59% 13.150% 3 16.534 2275 2290 2305 rBV 1778398 4733688 89.50% 16.673% 4 24.461 3621 3639 3655 rBV 1724006 4928503 93.18% 17.359% 5 27.533 4149 4162 4173 rBV4 182272 509335 9.63% 1.794%

6 31.076 4754 4765 4779 rBV3 13780 44607 0.84% 0.157% 7 31.717 4854 4874 4890 rBV2 1727279 5289185 100.00% 18.629% 8 31.958 4906 4915 4925 rVB4 15767 48419 0.92% 0.171% 9 39.931 6260 6272 6292 rBV2 2301109 4593865 86.85% 16.180% 10 43.151 6807 6820 6845 rBV2 1628037 3367781 63.67% 11.862%

Sum of corrected areas: 28392188

10301.D SCAN020507.M Tue May 14 14:26:53 2002 Page 1

NYC-WTC_000024929

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NYC-WTC_000024929Source: NYC Law Department, mirrored locally

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