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GCMS analysis results for sample AE10301, May 10, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10301 conducted on May 10, 2002, including surrogate recovery data.

NYC-WTC_000024927–000024934

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020509\10301.D Vial: 26 Acq On : 10 May 2002 11:20 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 10 13:30:00 2002 Quant Results File: SCAN020507.RE Quant Method Title Last Update Response via DataAcq Meth : : : : : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Method 508 GC/MS Scan Thu May 09 09:21:01 2002 Initial Calibration 508SCAN1 AA P Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 543901 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 2057342 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 1095505 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1875540 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1502821 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 959083 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.53 207 48403 5.53 ug/1 -0.04 Spiked Amount 10.000 Recovery = 55.30% Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10301.D SCAN020507.M Tue May 14 14:20:59 2002 Page 1

NYC-WTC_000024927

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NYC-WTC_000024927Source: NYC Law Department, mirrored locally

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