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GCMS analysis results for sample AE10245, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10245 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024863–000024870

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Quantitation Report (Q’L Reviewed) Data File : C:\MSDCHEM\l\DATA\020509\10245.D Vial: 23 Acq On : 10 May 2002 8:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 10 09:17:29 2002 Quant Results File: SCAN020507 .RE / Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 455129 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1714143 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.45 164 916178 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1562507 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1266097 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 827335 40.00 ug/1 -0.03 System Monitoring Compounds 27) TCMX 27.54 207 42385 5.79 ug/1 -0.04 Spiked Amount 10.000 Recovery = 57.90% Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10245.D SCAN020507.M Tue May 14 14:17:31 2002 Page 1

NYC-WTC_000024863

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NYC-WTC_000024863Source: NYC Law Department, mirrored locally

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