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GCMS analysis results for sample AE11304, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11304 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024596–000024612

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024598
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 0

Data File : C:\MSDCHEM\1\DATA\020516\11304.D Vial: 15 Acq On : 16 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 17 13:10:00 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 11.38 152 328543 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1223635 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.45 164 659107 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1118932 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 880364 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 508754 40.00 ug/1 -0.03 System Monitoring Compounds 27) TCMX 27.56 207 191892 36.45 ug/1 -0.02 Spiked Amount 40.000 Recovery 91.13% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 45262 2.40 ug/1 96

(#) = qualifier out of range (m) = manual integration (+) = signals summed 11304.D SCAN020507.M Fri May 17 13:11:05 2002 Page 1

NYC-WTC_000024598

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NYC-WTC_000024598Source: NYC Law Department, mirrored locally

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