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GCMS results for sample AE11482, May 29, 2002

Machine-extracted title · confidence 100%

Laboratory report of GCMS analysis for sample AE11482 conducted on May 29, 2002.

NYC-WTC_000022588–000022597

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020521\11482.D Vial: 16 Acq On : 21 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 09:37:26 2002 Quant Results File: SCAN020521.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Fri May 24 09:17:56 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 423946 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1601610 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.45 164 841428 40.00 ug/1 -0.03 3 0) Phenanthrene -d10 31.72 188 1430658 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1044575 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 589624 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.56 207 240753 35.67 ug/1 -0.04 Spiked Amount 40.000 Recovery 89.18% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.51 149 2736 0.12 ug/1 # 82

(#) = qualifier out of range (m) = manual integration (+) = signals summed 11482.D SCAN020521 .M Fri May 24 09:38:31 2002 Page 1

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NYC-WTC_000022590Source: NYC Law Department, mirrored locally

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