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GCMS analysis results for sample AE11303, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11303 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024585–000024595

Folder label: “GCMS X 5/13/02 A 5/16/02

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OCR text

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020516\11303.D Vial: 14 Acq On : 16 May 2002 10:12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.643 91 96 105 rVB4 12978 22312 0.74% 0.124% 2 6.152 510 523 573 rBV 521068 1159827 38.52% 6.421% 3 11.375 1400 1412 1436 rBV 836446 2156677 71.63% 11.941% 4 16.534 2275 2290 2310 rBV 1049221 2692238 89.42% 14.906% 5 24.460 3624 3639 3656 rBV 1012910 2801807 93.06% 15.512%

6 27.551 4144 4165 4178 rBV2 629268 1785530 59.30% 9.886% 7 31.082 4760 4766 4776 rVB3 5977 16677 0.55% 0.092% 8 31.717 4857 4874 4897 rBV2 1027031 3010842 100.00% 16.670% 9 31.958 4904 4915 4923 rVB4 8208 23708 0.79% 0.131% 10 39.931 6262 6272 6292 rBV2 1321157 2534360 84.17% 14.032%

11 40.518 6364 6372 6387 rBV2 51614 135560 4.50% 0.751% 12 43.151 6809 6820 6855 rBV 866775 1722260 57.20% 9.535%

Sum of corrected areas: 18061798

11303.D SCAN020507.M Fri May 17 13:09:43 2002 Page 1

NYC-WTC_000024589

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NYC-WTC_000024589Source: NYC Law Department, mirrored locally

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