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GCMS re-analysis comments for sample AE10519, May 29, 2002

Machine-extracted title · confidence 100%

Laboratory commentary regarding low recovery and subsequent re-analysis of sample AE10519 conducted on May 29, 2002.

NYC-WTC_000022609–000022618

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\l\DATA\020521\10519.D Vial: 9 Acq On : 21 May 2002 4:17 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 6.152 518 523 561 rBV 572002 1179737 26.26% 4.542% 2 11.370 1400 1411 1434 rBV 1233298 3231396 71.94% 12.442% 3 16.534 2272 2290 2309 rBV 1467155 4035529 89.84% 15.538% 4 24.460 3618 3639 3654 rBV 1461705 4212643 93.78% 16.220% 5 27.551 4144 4165 4182 rBV2 903317 2676800 59.59% 10.307% 6 28.908 4386 4396 4404 rVB5 8210 24672 0.55% 0.095% 7 31.088 4759 4767 4780 rBV3 11288 32064 0.71% 0.123% 8 31.717 4852 4874 4904 rBV2 1466214 4491876 100.00% 17.295% 9 31.952 4906 4914 4925 rVB5 12221 38001 0.85% 0.146% 10 39.931 6262 6272 6301 rBV2 1841316 3642789 81.10% 14.026% 11 43.151 6809 6820 6849 rBV2 1156144 2405946 53.56% 9.264%

Sum of corrected areas: 25971453

10519.D SCAN020521.M Fri May 24 09:20:33 2002 Page 1

NYC-WTC_000022612

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NYC-WTC_000022612Source: NYC Law Department, mirrored locally

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