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GCMS chain of custody form, sample AE10986, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10986 on May 22, 2002, including surrogate compound data.

NYC-WTC_000024450–000024462

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024454
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LC Area Percent Report

Data File : C: \MSDCHEM\1\DATA\020515\ 10986 .D Vial: 16 Acq On : 16 May 2002 2:37 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.643 88 96 102 rBV5 15753 30083 0.74% 0.122% 2 5.083 336 341 351 rBV3 23181 43987 1.09% 0.178% 3 6.117 512 517 520 rBV3 17581 29242 0.72% 0.119% 4 6.158 520 524 554 rVB 706449 1363505 33.76% 5.527% 5 11.376 1400 1412 1436 rBV 1163656 2930922 72.56% 11.880%

6 16.534 2277 2290 2307 rBV 1443979 3641907 90.16% 14.761% 7 24.460 3624 3639 3653 rBV2 1394952 3746639 92.75% 15.186% 8 27.551 4144 4165 4179 rBV2 851041 2363727 58.52% 9.581% 9 31.088 4759 4767 4781 rVB3 8716 31411 0.78% 0.127% 10 31.717 4853 4874 4896 rBV2 1360566 4039397 100.00% 16.372%

11 31.952 4906 4914 4929 rVB4 13182 46353 1.15% 0.188% 12 39.931 6261 6272 6290 rBV2 1791861 3470671 85.92% 14.067% 13 40.518 6363 6372 6388 rBV 226079 524766 12.99% 2.127% 14 43.151 6809 6820 6847 rBV 1202376 2409256 59.64% 9.765%

Sum of corrected areas: 24671866

10986.D SCAN020507.M Thu May 16 09:22:56 2002 Page 1

NYC-WTC_000024454

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NYC-WTC_000024454Source: NYC Law Department, mirrored locally

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