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GCMS blank analysis results for sample AE10851, May 2002

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Laboratory report showing GCMS blank analysis for sample AE10851 on May 20, 2002, listing compounds below method detection limits.

NYC-WTC_000024187–000024196

Folder label: “GCMS X 5/10/02 A 5/15/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY1502\LB.D Vial: 3 Acq On : 15 May 2002 4:02 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 17 9:07 2002 Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 10 09:59:40 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 0.00 178 0 N.D. 36) Di-n-butylphthalate 27.52 149 12282m 0.42 ug/1 3 7) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.06 149 340 N.D. 41) Benzo(a)anthracene 33.67 228 2186 N.D. 42) Bis(2-ethylhexyl)phthalate 33.84 149 1446 N.D. 43) Chrysene 33.67 228 2186 N.D. 45) Di-n-Octylphthalate 35.57 149 339 N.D. 46) Benzo(b)fluoranthene 36.67 252 1607 N.D. 47) Benzo(k)fluoranthene 36.72 252 1667 N.D. 48) Benzo(a)pyrene 37.64 252 816 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 43.11 276 189 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0510.M Fri May 17 09:08:04 2002 Page 2

NYC-WTC_000024189

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NYC-WTC_000024189Source: NYC Law Department, mirrored locally

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