GCMS blank analysis results for sample AE10851, May 2002

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Laboratory report showing GCMS blank analysis for sample AE10851 on May 20, 2002, listing compounds below method detection limits.

NYC-WTC_000024187–000024196

Folder label: “GCMS X 5/10/02 A 5/15/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY1502\LB.D Vial: 3 Acq On : 15 May 2002 4:02 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 17 9:07 2002 Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209625/TCLP calibration table Last Update : Fri May 10 09:59:40 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.16 152 344211 40.00 ug/1 -0.03 10) Naphthalene-d8 15.79 136 1372083 40.00 ug/1 -0.04 17) Acenaphthene-diO 21.10 164 669163 40.00 ug/1 -0.04 30) Phenanthrene-diO 25.54 188 942401 40.00 ug/1 -0.03 38) Chrysene-dl2 33.61 240 584310 40.00 ug/1 -0.03 44) Perylene-dl2 37.83 264 351637 40.00 ug/1 -0.03

System Monitoring Compounds 28) TCMX 23.24 209 128914 38.73 ug/L -0.03 Spiked Amount 40.000 Recovery 96.82% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis (2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0:00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Ac enapht hene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.57 149 1807 N.D. 26) 4-Chlorophenylphenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.24 168 202 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 0.00 178 0 N.D. (#) = qualifier out of range (m) = manual integration LB.D GCMS0510.M Fri May 17 09:08:04 2002 Page 1

NYC-WTC_000024188

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GC/MS blank analysis results, sample AE09683, May 9-10 2002 · Box DEP Box 18

NYC-WTC_000023551

Laboratory report showing GC/MS blank analysis for sample AE09683 with non-detect results for volatile organic compounds.

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