GCMS comments for sample AE10206 re-extraction, May 2002

NYC 9/11 Public Portal Document ICDW

Data File : C:\MSDCHEM\1\DATA\051602\10206.D Vial: 7 Acq On : 16 May 2002 7:25 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.109 3 5 14 BV 4 2820 33002 ' 0.07% 0.011% 2 3.308 35 39 44 PV 4 6048 76620 0.15% 0.026% 3 3.361 44 48 74 W 4 3226 88813 0.18% 0.031% 4 3.526 74 76 80 PV 4 1917 25154 0.05% 0.009% 5 3.596 83 88 94 W 12985 221266 0.44% 0.076%

6 3.726 101 110 124 W 2 7004 276938 0.56% 0.095% 7 4.143 176 181 194 W 7 3012 93472 0.19% 0.032% 8 4.243 194 198 203 W 4 3007 50324 0.10% 0.017% 9 5.030 325 332 337 PV 7 3402 83962 0.17% 0.029% 10 5.077 337 340 350 W 9 3407 97566 0.20% 0.034%

11 5.341 378 385 390 W 7 2157 58045 0.12% 0.020% 12 5.406 390 396 401 W 5 4204 107420 0.22% 0.037% 13 5.559 418 422 424 PV 4 1698 21089 0.04% 0.007% 14 5.594 424 428 430 W 3 2079 35114 0.07% 0.012% 15 5.635 430 435 444 W 5 3123 83428 0.17% 0.029%

16 5.970 484 492 519 W 787791 14350368 28.77% 4.943% 17 6.140 519 521 526 W 5 3029 47189 0.09% 0.016% 18 7.727 786 791 804 PV 3 8510 211281 0.42% 0.073% 19 8.743 959 964 973 W 3 3606 77288 0.15% 0.027% 20 8.826 973 978 984 PV 5 1669 30407 0.06% 0.010%

21 9.301 1055 1059 1069 PV 4 1967 41614 0.08% 0.014% 22 9.936 1158 1167 1184 W 1770479 33579353 67.33% 11.568% 23 10.200 1206 1212 1218 W 6 2383 36670 0.07% 0.013% 24 10.259 1218 1222 1232 PV 6 2910 62098 0.12% 0.021% 25 10.388 1235 1244 1247 PV 7 1397 25690 0.05% 0.009%

26 12.034 1520 1524 1530 W 2 2650 46068 0.09% 0.016% 27 12.404 1576 1587 1593 BV 5 2281 38908 0.08% 0.013% 28 12.909 1662 1673 1679 PV 6 2746 73942 0.15% 0.025% 29 13.197 1716 1722 1729 BV 2 4916 89047 0.18% 0.031% 30 13.432 1752 1762 1783 PV 2419711 45224292 90.67% 15.579%

31 13.579 1783 1787 1793 W 6863 112850 0.23% 0.039% 32 15.700 2140 2148 2155 PV 3 2201 37909 0.08% 0.013% 33 16.746 2321 2326 2332 PV 4 3692 65297 0.13% 0.022% 34 17.151 2382 2395 2402 PV 6 9044 145035 0.29% 0.050% 35 17.657 2472 2481 2486 BV 3 3881 56116 0.11% 0.019%

36 18.567 2625 2636 2654 PV 2558871 49876177 100.00% 17.182% 37 18.967 2695 2704 2709 W 2 1677 40224 0.08% 0.014%

10206.D 050102.M Fri May 17 15:02:32 2002 Page 1

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