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GC/MS reference standard results for nitrosamines, sample AE10895, May 20

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Laboratory report showing reference standard analysis results for nitrosamines and other compounds in sample AE10895.

NYC-WTC_000024062–000024069

Folder label: “GCMS X 5/10/02 A 5/16/02

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NYC 9/11 Public Portal Document yuai-A LCL LOIl KepOrC (QT Revlewed)

Data File : C:\MSDCHEM\1\DATA\051602\510REF2.D Vial: 5 Acq On : 16 May 2002 5:48 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 17 15:10:14 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 7721157 16.29 ug/L 99 3 8) Pyrene 27.17 202 8096667 17.93 ug/L 97 39) Butylbenzylphthalate 29.52 149 2341005 11.63 ug/L # 96 40) Benzo(a)anthracene 30.78 228 5337819 14.84 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.38 149 2865587 10.54 ug/L 96 42) Chrysene 30.87 228 6414718m 17.23 ug/L 44) Di-n-octylphthalate 33.23 149 2710835 8.55 ug/L 99 45) Benzo(b)fluoranthene 33.74 252 4391716 16.89 ug/L 97 46) Benzo(k)fluoranthene 33.82 252 5713593 17.48 ug/L 99 47) Benzo(a)pyrene 34.55 252 2372665 9.14 ug/L 98 48) Indeno(1,2,3-cd)pyrene 37.38 276 1903624 10.46 ug/L 99 49) Dibenz(a,h)anthracene 37.50 278 2655333 13.72 ug/L 99 50) Benzo(g,h,i)perylene 38.12 276 3077398 15.14 ug/L 100

(#) = qualifier out of range (m) = manual integration (+) = signals summed 510REF2.D 050102.M Fri May 17 15:10:50 2002 Page 2

NYC-WTC_000024068

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NYC-WTC_000024068Source: NYC Law Department, mirrored locally

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