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GC/MS blank analysis results, sample AE09676, May 20-21 2002

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Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.

NYC-WTC_000023649–000023661

Folder label: “GCMS X 5/9/02 A 5/20/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2002\LB.D Vial: 6 Acq On : 20 May 2002 11:06 am Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 20 15:19 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.15 152 337924 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 1333721 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.08 164 622959 40.00 ug/1 0.00 30) Phenanthrene-diO 25.52 188 818792 40.00 ug/1 -0.02 38) Chrysene-dl2 33.57 240 472793 40.00 ug/1 -0.03 44) Perylene-dl2 37.79 264 308348 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.23 209 115518 36.90 ug/L 0.00 Spiked Amount 40.000 Recovery 92.25% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.19 146 105 N.D. 5) 1,4-Dichlorobenzene 12.19 146 105 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene o'. 00 180 0 N.D. 15) Naphthalene 15.83 128 644 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.57 149 439 N.D. 26) 4-Chlorophenylphenylether 23.23 204 460 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.59 178 520 N.D. (#) = qualifier out of range (m) = manual integration LB.D GCMS0520.M Mon May 20 15:19:54 2002 Page 1

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NYC-WTC_000023650Source: NYC Law Department, mirrored locally

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