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GCMS analysis results, sample AE09398, May 2002

Machine-extracted title · confidence 78%

Gas chromatography-mass spectrometry analysis of sample AE09398 conducted May 15, 2002, with surrogate 2,4-DDD recovery at 79 percent.

NYC-WTC_000023635–000023645

Folder label: “GCMS X 5/9/02 A 5/10/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY1002\9398.D Vial: 6 Acq On : 10 May 2002 5:56 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 13 9:08 2002 Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 13 08:58:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.55 178 409 N.D. 36) Di-n-butylphthalate 27.53 149 9969 N.D. 37) Fluoranthene. 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.05 149 395 N.D. 41) Benzo(a)anthracene 33.62 228 3338 N.D. 42) Bis(2-ethylhexyl)phthalate 33.85 149 12474 0.56 ug/1 # 98 43) Chrysene 33.69 228 1302 N.D. 45) Di-n-Octylphthalate 35.59 149 1256 N.D. 46) Benzo(b)fluoranthene 36.67 252 1176 N.D. 47) Benzo(k)fluoranthene 36.74 252 1987 N.D. 48) Benzo(a)pyrene 37.65 252 597 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 43.15 276 389 N.D.

(#) = qualifier out of range (m) = manual integration 9398.D GCMS0510.M Mon May 13 09:12:10 2002 Page 2

NYC-WTC_000023638

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NYC-WTC_000023638Source: NYC Law Department, mirrored locally

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