GCMS analysis results for sample AE10160, May 2002

NYC 9/11 Public Portal Document

s Data File : C:\MSDCHEM\1\DATA\051302\10160.D Vial: 10 Acq On : 13 May 2002 6:49 pm Operator: Mclean Sample : 5/9 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 3-Hexen-2-one Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

5.03 0.22 ug/L 177600 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexen-2-one 98 C6H10O 000763-93-9 64 2 2-Heptene, (E)- 98 C7H14 014686-13-6 20 3 2-Pentene, 2,3-dimethyl- 98 C7H14 010574-37-5 9 4 3,4-Dimethyl-2-pentene(c,t) 98 C7H14 1000118-16-5 9 Abundance Scan 332 (5.030 min): 10160.D (-326) (-) m/z 83.10 100. 00% 83 55

5000 98 43 49 4-4- m/z-> Ol .II. 10 20 30 40 50 "Tl 1 1 1 । । 1 1 1 1 । । 60 70 80 88 - 90 1 I 1 1 100 4.60 4.80 5.00 5.20 5.40 m/ Z 55.20 69.66% Abundance #116424: 3-Hexen-2-one 83 55 5000 43 98 4.60 4.80 5.00 5.20 5.40 m/z 98.00 42.81% 50 । , 63 69 77 m/z-> 0+ ...... ■ .pl1! +TTTT +93 10 20 30 40 50 60 70 80 90 100 Abundance #13656: 2-Heptene, (E)- 55 41 27 4.60 4.80 5.00 5.20 5.40 5000 69 98 m/z 43.15 33.47%

15

m/z-> 01 - 10 20 30 40 —505l 60 70 77 83 91 * * r* ■ ■ ■ ] 1 * 80 90 100 I ’ 1 MAnampopy/ VWwuA Abundance #32863: 2-Pentene, 2,3-dimethyl- i r ■ ' 1 i ' 1 55 83 4.60 4.80 5.00 5.20 5.40 41 m/z 39.10 29.75% 5000 27 98 69 15

m/z-> 0 — 10 L20 All30 . 36,/401444 50 1.1,83,0,17 60 70 7744 80 +91 I 1 ' 90 100 A/AAA AA— I ■ ■ > > I 1 ’ 1 1 r 1 4.60 4.80 5.00 5.20 5.40

10160.D 050102.M Tue May 14 11:40:40 2002 Page 5

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