GCMS Method 508 scan results, April 2002

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' Data File : C:\MSDCHEM\l\DATA\020419\08487.D Vial: 24 Acq On : 20 Apr 2002 6:46 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C: \DATABASE\ni s 198.1 Peak Number 4 2-Propanone, 1,1-dichloro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.12 0.51 ug/1 666781 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 23 2 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 9 3 Ethanone, 1-(1,4,5,6-tetrahydro- ... 125 C7H11NO 1000248-99-2 7 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 Abundance Scan 518 (6.123 min): 08487.D (-510) (-) m/ z 43.10 100.00% 43

5000 . — j । । i । ।

5.80 6.00 6.20 6.40 35 . Of mPPPTH 49 61.. 83. 97,110 117 12 ''' 111,1 I111 1 I ‘ 1 1 1 1 111' I ' 1 1 'I ’ ’’1’’ । । > ’411.01 m/z 125.00 9.73% niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3861: 2-Propanone, 1,1-dichloro- 4

5000 • • ’ । > ■ ■ ■ । f ■ । i > j 1 । । ■ I 5.80 6.00 6.20 6.40 m/z 127.00 6.65% 15 27I . 36 , 49 55 63 1 | ' ’761 ■ | 83 93 125 01 TIBiiji rlr) ' * 1 ‘ 1 1 1 • • > l ) ■ ' | । fl ■ . I I . i i r-|' ■ 1 1 1 I 1 1 1 1 1"' 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3877:2-Propanone, 1,1,1-trichloro- 43 r। < t • ■ . > । 5.80 6.00 6.20 6.40 5000 m/z 83.00 5.88%

15 1 27 36 . ,4? 55 63 O+ TIT++ 76 83 91 97 110117 125 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #6868: Ethanone, 1 -(1,4,5,6-tetrahydro-2-pyridinyl)- M1nAr 1 m । meii 43 5.80 6.00 6.20 6.40 54 82 m/z 97.00 5.01%

5000 125

68 97 - 110 0 । ' I ' 4 1 PTTT — —IPPT .................... m/z—> 10 20 30 40 60 70 80 90 100 110 120 130 5.80 6.00 6.20 6.40TT

08487.D SCAN020418.M Mon Apr 29 08:36:51 2002 Page 22

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