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GCMS analysis results for sample AE08430, May 2002

Machine-extracted title · confidence 90%

Laboratory report listing concentrations of unknown compounds and surrogates in sample AE08430 analyzed on May 16, 2002.

NYC-WTC_000023228–000023237

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File C:\HPCHEM\1\DATA\MAY0 902\8430.D Vial: 10 * Acq On 9 May 2002 11:13 pm Operator: Sample GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.161 337 341 370 rBV 684354 1492333 39.59% 7.194% 2 12.193 775 781 798 rBV 1177813 2671996 70.88% 12.881% 3 14.796 1057 1065 1072 rBV 56321 107155 2.84% 0.517% 4 15.822 1171 1177 1194 rBV 1593871 3383130 89.74% 16.310% 5 21.137 1750 1757 1780 rBV 1759102 3769866 100.00% 18.174% 6 23.272 1981 1990 1996 rBV 773332 1587053 42.10% 7.651% 7 25.572 2234 2241 2252 rBV2 1576250 3494902 92.71% 16.848% 8 33.636 3114 3121 3132 rBV 1094575 2452997 65.07% 11.826% 9 37.860 3574 3582 3602 rBV2 611358 1783791 47.32% 8.599%

Sum of corrected areas: 20743223 8430.D GCMS0510.M Fri May 10 13:57:28 2002

NYC-WTC_000023233

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NYC-WTC_000023233Source: NYC Law Department, mirrored locally

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