NYC-WTC_000024014
Laboratory report showing GC/MS analysis of sample AE10985 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Document / 32 pages
GCMS analysis results for sample AE09571, May 2002
Machine-extracted title · confidence 100%Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.
NYC-WTC_000023023–000023054Folder label: “GCMS X 5/8/02 A 5/9/02”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb- Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Cyclohexane, 1,2,4,5-tetrae.. Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 32.32 1.48 ug/L 2566190 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexane, 1,2,4,5-tetraethyl- 196 C14H28 061142-00-5 27. 2 Spiro[4.5]decane-1,6-dione 166 C1OH1402 036803-48-211 3 Pyrrolidine, 1-(1-propenyl)- 111 C7H13N 013937-88-710 4 Cyclohexane, 1,2,4-trimethyl- , (. . . 126 C9H18 007667-60-9 10 Abundance Scan 4976 (32.316 min): 9570. D (-4966) (-) m/z 55.15 700.00%
43 55 83 111 povor"man-#M""“M 5000 71 150 167 135 208 98 123 181 261 276 — 32.00 32.20 32.40 32.60 0! TIB ■111 i । TIf — 1 ■ i 1 ■ 1 ■ i ■ ' 1 ■ i ' ' TT m/z 111.10 76.66% miz-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 55 69 #13957: Cyclohexane, 1,2,4,5-tetraethyl- 97 111 pwyhyMdt“rW"M 83 41 5000 167 32.00 32.20 32.40 32.60 29 125 m/z 83.10 68.88%
m/z-> OlTIT
Abundance :20 — 40 44 60 —4 L 154 — 183 196 . , 1-i , I a ,137 80 100 120 140 160 180 200 220 240 260 280 #120086: Spiro[4.5]decane-1,6-dione 11111-*t*I**’’I’*/*/I AAAwyeytanhy 44 1 1
32.00 32.20 32.40 32.60 67 m/z 43.10 61.61% 5000 95 138 166
. l | I | | | ■ I | | | | | | | | | | | | | | | | | | 1 | | |-| I r i i-| ! 0 i ■■ ■■i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #50410: Pyrrolidine, 1-(1-propeny!)- 1 1 32.00 32.20 32.40 32.60 43 m/z 41.20 45.54% 5000 55 71 96 mMyWnyMHAp 28 83 —— 0 TTT TH ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 32.00 32.20 32.40 32.60
9570.D 050102.M Mon May 13 11:46:48 2002 Page 19
NYC-WTC_000023046
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