Laboratory report of a GCMS blank run conducted on May 14, 2002, showing non-detect results for various compounds.
NYC-WTC_000022965–000022989Folder label: “GCMS X 5/8/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document X WL ULIU ICD —
Data File C:\MSDCHEM\1\DATA\050902\0508LB.D Vial: 4 Acq On 9 May 2002 5:43 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 Cyclononasiloxane, octadeca... Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
36.50 1.60 ug/L 1032610 Perylene-d12 34.70
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 87 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 53 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 43 4 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 32 Abundance Scan 5688 (36.499 min): 0508LB.D (-5674) (-) m/ z 73.10 100.00% 73 147 221
5000 281 _ I I I I I I I _
355 429 36.20 36.40 36.60 36.80 0- I'' 40 ■ ' i' t+t 191 | 11,3251,1 ■ ■ 11 ■ I 1 503 m/z 147.10 80.95% m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429
355 5000 281 IIIIIYi 1MA" . AMMrimM e 36.20 36.40 36.60 36.80 m/z 221.10 70.89%
n/z-> 0- । । I ’ 1 1 ' I 1 1 50 ' ' I ' r ' I ' ' r' l ‘ MLTT 100 150 200 250 300 350 400 450 500 550 600 650 —TTTT 651 475
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)... 73 I+IIIIIIruI"Autsus 147 36.20 36.40 36.60 36.80 5000 267 m/z 281.10 39.03% 355 429 207
0- 1 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 woMAompnt Wwlyntww Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 73 147 36.20 36.40 36.60 36.80 m/z 207.00 30.38% 281 / 5000
369
/z-> 0 2744 50 117 Tff 177^ 249,
100 150 200 250 nu" epertihr 338 I 1 1 ' ■ ■ ■ i ' 300 350 400 450 500 550 600 650 36.20 36.40 36.60 36.80
0508LB.D 050102.M Tue May 14 10:15:01 2002 Page 18
NYC-WTC_000022986
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NYC-WTC_000024041
Laboratory report showing non-detectable levels of nitrosamines and other contaminants in blank sample AE10895.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025216
Laboratory report showing GCMS blank analysis for sample AE11410 conducted on May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023409
Laboratory report showing non-detect results for volatile organic compounds in a method blank sample AE10137 analyzed on May 14, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023925
Laboratory report showing GC/MS analysis of sample AE10982 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023991
Laboratory report showing GC/MS analysis of sample AE10984 with surrogate recovery data for 2,4-DDD.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025102
Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023949
Laboratory report showing GC/MS analysis of sample AE10983 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045936
Gas chromatography-mass spectrometry blank analysis conducted May 17, 2002 testing for semivolatile organic compounds with all results below method reporting limits.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044559
Laboratory report showing blank test results for various organic compounds on May 7, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013883
Fragmented document header from DEP Box 15 archive containing metadata for environmental testing records dated late May 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046006
Gas chromatography-mass spectrometry report for sample AE10810 showing detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044381
Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for organic compounds.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000022961
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000022962
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder
NYC-WTC_000022990
Laboratory report documenting GCMS calibration verification analysis conducted on May 14, 2002.
Filed in the same folder
NYC-WTC_000022994
Laboratory report of GCMS reference standard analysis conducted on May 14, 2002, showing recovery percentages.
Filed in the same folder
NYC-WTC_000023002
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder