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GCMS calibration data for TCLP method, May 2002

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000022909–000022915

Folder label: “GCMS X 5/8/02 A 5/10/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C: \HPCHEM\ 1 \DATA\MAY0 302\9332.D Vial: 34 Acq On 5 May 2002 12:22 am Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 11:52 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue 3 5) Anthracene 25.63 178 298 N.D. 3 6) Di-n-butylphthalate 27.55 149 4225 N.D. 37) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.08 149 1176 N.D. 41) Benzo(a)anthracene 33.63 228 1718 N.D. 42) Bis(2-ethylhexyl)phthalate 33.86 149 100493 5.07 ug/1 99 43) Chrysene 33.63 228 1718 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.87 252 2102 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 9332.D GCMS0501.M Tue May 07 11:52:39 2002 Page 2

NYC-WTC_000022910

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NYC-WTC_000022910Source: NYC Law Department, mirrored locally

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