NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Vial: 40
Data File : C : \HPCHEM\ 1 \DATA\MAY2 102 10601.D
Acq On : 23 May 2002 5:01 am ' <3002
Operator:
Sample : EXTRACT5/20 lit0' 3 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: May 24 8:30 2002 Quant Results File: GCMS0520.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update
Response via
DataAcq Meth
:
:
:
Mon May 20 15:10:30 2002
Initial Calibration
GCMS0520
N"
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.14 152 442771 40.00 ug/1 0.00
10) Naphthalene-d8 15.77 136 1738598 40.00 ug/1 -0.02
17) Acenaphthene-diO 21.09 164 833399 40.00 ug/1 0.00
30) Phenanthrene-diO 25.53 188 1092035 40.00 ug/1 0.00
38) Chrysene-dl2 33.60 240 629544 40.00 ug/1 -0.01
44) Perylene-dl2 37.82 264 420149 40.00 ug/1 0.02
System Monitoring Compounds
28) TCMX 23.23 209 160790 38.39 /g/L . 00
Spiked Amount 40.000 Recovery = ( 95.97%
Target Compounds Qvalue
2) N-nitrosodimethylamine 0.00 74 0 N.D. X
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 14.49 82 1644 N.D.
13) bis(2-Chloroethoxy)methane 15.16 93 235 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.83 128 412 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0,. 00 162 0 N.D.
20) Dimethylphthalate 20.44 163 789 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Ac enapht hylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.57 149 1516 N.D.
26) 4-Chlorophenylphenylether 23.23 204 623 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzene 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 23.23 168 422 N.D.
32) 4-Bromophenylphenylether 0.00 248 0 N.D.
33) Hexachlorobenzene 0.00 284 0 N.D.
3 4) Phenanthrene 25.60 178 736 N.D.
(#) = qualifier out of range (m) = manual integration
10601.D GCMS0520.M Fri May 24 08:30:46 2002 Page 1
NYC-WTC_000022709
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