GCMS unknowns analysis, sample AE11604, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \HPCHEM\ 1 \DATA\MAY2 102\11604.D Vial: 33 Acq On : 22 May 2002 10:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.12 18.13 ug/1 1062120 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2 7CHCH2C (0) OCH3 100 C5H802 003724-55-8 9 3 Ace?rone 58 C3H60 000067-64-1 7 4 57H exen-2-one 98 C6H10O 000109-49-9 7 Abundance Scan 336 (8.119 min): 11604.D (-) m/z 43.05 100.00%| 43

5000 59 ' I ' ' 1 1 i ' 1 1 rI ' l 11 11 I . 101 7.80 8.00 8.20 8.40 ............................................. 38 I 1 1 I 1 11 1 I 1 1 1 1 I 1 ' 1 ' 1 1 11153. ' i 1 69 ' ' 1 i ■ ■ ■ ' i 83 1 ' ■ ■ i ' 1 1 1 i 1 ■ ' ' i ' m/z 59.10 38.50% m/z—> 10 20 30 40 50 160 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 m/z 58.10 16.77% 27 101

miz-> I I i ■ ■ ■ ■ i 1 ' ■ ■ i ' 10 20 30 T+ 40 49 ,, 11111 50 83 m3 1 । 1 1 1 1 I 111 1 1 । 60 70 80 90 + 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 ' 1 ■ । ■ ■1 11 1 FrI i 1Ln i 1 1 1 1 । 7.80 8.00 8.20 8.40 5000 m/z 101.15 12.60%

58 ................... 38 ............. .............. I. 100 i ■ ■ 1 'I 1 1 1 1 1T4 1 1 r1 ' i ■ ' 1 1 i ■ ■ ■ ■ I ■ ' ■ 1 i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone 43 7.80 8.00 8.20 8.40 m/z 41.15 6.47% 5000 15 58 27 1 1 1 I l, ' 1 1 ' r 1 1 ' i 1 1 i ' ■ ' 1 i ■ ■ ‘ 1 i ' 1 ■ ■ i ■ 1 ■ ■ i ' ■ ■ ■ i ■ . । j r i "ITT > i > । m/z— > 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

11604.D GCMS0520.M Fri May 24 08:33:48 2002 Page 1

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