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Volatile organic compounds results, Mar 14 2002

Machine-extracted title · confidence 95%

Laboratory analysis results for volatile organic compounds sample AE06052 dated March 14, 2002.

NYC-WTC_000021748–000021851

Folder label: “524 3/14/02

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Scanned page image, NYC-WTC_000021803
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02MAR08\5172.D Vial: 9 Acq On 8 Mar 2002 4:55 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 Propanoic acid Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

17.20 0.04 ug/L 7860 1,4-DIFLUOROBENZENE 15.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanoic acid 74 C3H602 000079-09-4 2 2 N-Nitrosodimethylamine 74 C2H6N20 000062-75-9 2 3 2(5H)-Furanone 84 C4H4O2 000497-23-4 2 4 3-Hexene, (Z)-____________________________ 84 C6H12 ________ 007642-09-3 2 Abundance Scan 777 (17.197 min): 5172.D(-) m/z 73.95 100.00% 74

8000

6000 ,, , i, i,,,, ,,, , 82 16.80 17.00 17.20 17.40 17.60 TTTTTpTTTpTTTpTTTpTTTpTTTpTTTp-rTTyT^^ m/z 82.00 51.21% I’I* m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62559: Propanoic acid 74 45

5000 i ■ ■ ■ ‘ i ■ ■ i ■ ■ ' ■ i ' ■ ■ ' i ■ ‘ 16.80 17.00 17.20 17.40 17.60 57 m/z 84.00 41.31% A 40 |lI.>|II■■|IIU |.III|.II.|IU1|1■I I[.H1 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62544: N-Nitrosodimethylamine 42 74 I • ‘ ■ I ■R T 16.80 17.00 17.20 17.40 17.60 5000 15 30

I’TmltZRmmp HmmFslrpmmp mmmmppm m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #537:2(5H)-Furanone 55 84 27 5000

38 i""r,,,r,“r mmlpmmmp WpT m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90

5172.D HP022702.M Sun Mar 10 13:06:16 2002 Page 1

NYC-WTC_000021803

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NYC-WTC_000021803Source: NYC Law Department, mirrored locally

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