VOC analysis results, sample AE02089, Feb 7 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02feb06\2094.D Vial: 7 Acq On 6 Feb 2002 8:51 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins — Mise Multiplr: 1.00 MS Integration Params: LSCINT.P - Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Propanoic acid, methyl ester Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

13.06 0.02 ug/L 19143 1,4-DIFLUOROBENZENE 15.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanoic acid, methyl ester 88 C4H802 000554-12-1 9 2 Hydrazine, butyl- 88 C4H12N2 003530-11-8 4 3 1,2-Ethanediamine , N,N’-dimethyl- 88 C4H12N2 000110-70-3 3 4 Butane, 1-methoxy-_______________ 88 C5H120 000628-28-4 3 Abundance Scan 527 (13.059 min): 2094.D(-) m/z 57.05 100.00% 57 8000

6000 12.80 13.00 13.20 13.40 4000 88 m/z 88.10 38.40% ■ ■ i " ' ■ i ■ ■ ■ ■ i ■" ■ i ■' ■ ■ i1 ■'11" ■ ■ i1 ■ ■ ■ i ■ ■ •i■■■■i■■■■i ■' ■ ■ i ■' ■ • i ■ “ ■ i ■ ■ ■ • i ■ • ■ > i ■■ miz-> 2025303540455055 60 65 70 75 80 85 90 95 Abundance #807: Propanoic acid, methyl ester 23 57

5000 1280 13.00 1320 1340 88 m/z 59.05 38.03%

Hl-m# +9 26 ,33 45 " ।। ■ ■ ■' । ■1 ■ ■ । ■ ■ ■ ■ । ■1 ■ i" " i " N mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #837: Hydrazine, butyl- 41 56

73 12.80 13.00 13.20 13.40 5000 29 88 59 •' i ■1 ■ ■ i ■ ■ ■ ■ i ■ i ■ ■ ■ ■ i''1' i " ■ i1 ■ ■ ■ i ■1 niz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #833:1,2-Ethanediamine, N,N‘-dimethyl- 44

5000

58 41, -11175514 mmmm 74 88 ' i • ■■ ■ i ■■•11■ ■ " i" ■ ‘ i ■'1 ■i■■‘111 mfz~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

2094.D HP013102.M Wed Feb 06 21:32:23 2002 Page 1

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