Volatile organic compounds results, Mar 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02MAR20\6047A.D Vial: 13 Acq On : 20 Mar 2002 10:31 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : March 20, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 4-Heptanone Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.78 0.03 ug/L 19204 1,4-DIFLUOROBENZENE 15.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Heptanone 114 C7H140 000123-19-3 4 2 3-Hexanone, 2-methyl- 114 C7H140 007379-12-6 4 3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 4 4 3-Pentanone, 2,4-dimethyl- 114 C7H140 _________000565-80-0 3 Abundance Scan 694 (15.783 min): 6047A.D (-) m/z 114.15 100.00% 1 4 8000

6000

4000 63 88 15.40 15.60 15.80 16.00 ■ ■ i ■ ■' ■ i ■ ■ ■ • i'1 ■ ■ i ■' ■ ■ 11 p-rVrp-r-r-r-p-rTT-t-p-rr ' i ■ ' ■1 i ■ m/z 88.00 26.10% • ‘ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #64152:4-Heptanone 43 71

5000 27 It 15.40 15.60 15.80 16.00 m/z 63.05 24.66%

+ 114 58 99 | m/z-> ..... ...M.... 1 10 20 30 40 TIt lasa****1**4444**1*0**** 50 60 70 80 90 100 110 120 Abundance #64191:3-Hexanone, 2-methyl- 43

15.40 15.60 15.80 16.00 71 m/z 56.95 20.44% 5000 27 114 , 55 — mTPTTt m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #2826:3-Cyclobutene-1,2-dione, 3,4-dihydroxy- ■p-rr-rp-r ■n-p-n-p-r 29 15.40 15.60 15.80 16.00 58

5000 114

86 17 40 68 -PH 1■i■■ ■ ■ I'1 ‘111' p-r-r-rp-o-rp-r ‘ I ‘ ' ‘ ' I ‘ ‘ ' I ‘ ■n-pn m/z--> 10 20 30 40 50 60 70 80 90 100 110 120

6047A.D HP031802.M Fri Mar 22 09:51:30 2002 Page 1

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