VOC analysis results, sample AE03944, Feb 20 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB20\03944.D Vial: 10 Acq On : 20 Feb 2002 4:12 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 20, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ******************************************** ** *********************** Peak Number 4 3-Pentanone, 2,4-dimethyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 15.78 0.04 ug/L 39280 1,4-DIFLUOROBENZENE 15.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanone, 2,4-dimethyl- 114 C7H140 000565-80-0 3 2 4-Heptanone 114 C7H140 000123-19-3 3 3 3-Hexanone, 2-methyl- 114 C7H140 007379-12-6 3 4 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2!006843-45-4 3 Abundance Scan 693 (15.784 min): 03944.D (-) m/z 114.05 100.0041 1 4

5000 63 88 !1''’I’ '‘ I T IT 15.40 15.60 15.80 16.00 50 57 ■ i ' ■ ■ ■ i ■ ' 1 ' i ■ ■ ■ ■ I • ■ ' ■ i ■ ■ ' ■ i ' ■ ‘ ■ i ■ ■ m/z 63.05 27.94 1 I ' ‘ ‘ I ‘ ‘ ‘ I ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64142: 3-Pentanone, 2,4-dimethyl- 43

5000 71 15.40 15.60 15.80 16.00 m/z 88.10 23.29%

mlz-> —L 20 27

30 1"I 40 50 55 । I " " I'1 60 70 80 90 100 110 114 120 Abundance #64152:4-Heptanone 43 71 15.40 15.60 15.80 16.00 5000 m/z 50.05 14.52 27

114 58 ............. 11 ■ l - TTI . ......... 99..... 1.... +......................................... m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #3058:3-Hexanone, 2-methyl- 1*’**!’ T TTT 43 15.40 15.60 15.80 16.00 71 m/z 56.95 12.59

5000

27 . 114

m/z—> 20 30 40 -PP 50 55 60 ■ i1 ■ ■' i ■ ■ ■ ■ i ■ • ‘ ■ i ■ ■ • ■ i ■

70 80 90 100 110 120 i ■ ■ ■ ■ i ■ ■ L 15.40 15.60 15.80 16.00

03944.D HP021702.M Fri Feb 22 09:25:53 2002 Page 4

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