Volatile organic compounds results, Mar 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02MAR10\5232.D Vial: 5 Acq On : 10 Mar 2002 5:46 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolan-2-one Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.75 0.03 ug/L 18481 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dioxolan-2-one 88 C3H403 000096-49-1 3 2 Sulfide, allyl methyl 88 C4H8S 010152-76-8 3 3 1,2-Hydrazinedicarboxaldehyde 88 C2H4N202’ 000628-36-4 3 4 Hydrazine, 1,2-diethyl- 88 C4H12N2 ______ 001615-80-1 3 Abundance Scan 692 (15.749 min): 5232.D (-) m/z 114.15 100.00% 1 4

5000

■ i ■ ■ ' ‘ i ' 1’1141111 83 88 15.40 15.60 15.80 16.00 ___________ 44_____ |______ — m/z 63.05 21.63% 1' 111 '' 111'' 111 ■ ■ i ■ ■ • ■ i ■ ■ ■ ‘ i ■1 ‘ ■ i ■ ■ ■ ■ i ■ ■ ‘ I ‘ ‘ ' I ' TiT-n m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #82893:1,3-Dioxolan-2-one 29

43 88

5000 15.40 15.60 15.80 16.00 15 m/z 88.00 19.97% 58

m/z-> — 10 20 30 —P I'.. I ■ ■ .1, r 40 50 60 70 80 73 • i* i» * I ‘ ‘ 90 ‘ I ‘ ‘ * 1 1 ‘ ‘ ‘ I * ‘ 100 110 120 Abundance #62927: Sulfide, allyl methyl 41

73 88 15.40 15.60 15.80 16.00 5000 m/z 43.95 8.80%

61 MWMAooow m/z-> ■■i11■11 ■ ■ ‘' i ■11 ‘I' 10 48,....77... 2030405060 70 8090 100 ■ i ' ‘ ■ 1 i ■ ■ ‘ ' l ' 1 110 120 Abundance #781: 1,2-Hydrazinedicarboxaldehyde 31 15.40 15.60 15.80 16.00

60 88 5000 44 17 .. I , -Hp ■ ■ i ‘ ‘111' ‘ m/z--> 10 20 30 40 50 60 70 80 90 100 110 120

5232.D HP022702.M Mon Mar 11 11:23:29 2002 Page 1

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