Volatile organic compounds results, Mar 7 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\02mar07\5167.D Vial: 16 Acq On 7 Mar 2002 10:17 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxolan-2-one Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 15.72 0.03 ug/L 25370 1,4-DIFLUOROBENZENE 15.05 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dioxolan-2-one 88 C3H403 000096-49-1 3 2 Sulfide, allyl methyl 88 C4H8S 010152-76-8 3 3 1,2 -Hydraz inedicarboxaldehyde 88 C2H4N2021 000628-36-4 3 4 Hydrazine, 1,2-diethyl- 88 C4H12N2 001615-80-1 3 Abundance Scan 689 (15.715 mln): 5167.D (-) m/z 114.15 100.00% 1 14

5000 W.......... . 63 88 15.40 15.60 15.80 16.00 44 | # ■n-pn m/z 88.10 19.97% ■ • i11 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ • ■ ■ i ■ ■ ■ ■ i ■ ■ ■' i •'1 ■ 11 11I“1'I' / ti/z--> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62893:1,3-Dioxolan-2-one 29

43 88

5000 ■ ‘ i •' ■ ■ i ' ■ • i 1 ■ ■ ■ i ■ ■ ■ ' i 15.40 15.60 15.80 16.00 15 m/z 63.05 16.67% A 58 , T.....• I73 PTmTTT — ‘ » I » » * * | ...... ’ ‘ ‘ | ‘ Y 1154***4**1**I m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62927: Sulfide, allyl methyl 41 1 1 i ‘ >1 73 88 15.40 15.60 15.80 16.00 m/z 43.95 8.98% 5000

61 WW/WW m/z-> '‘I ■ ‘ ‘'I■' ‘ ‘ I‘‘ • ’I* 10 20 30 40 4441 mmmmmp 50 60 70 80 90 100 110 120 Abundance #781:1,2-Hydrazinedicarboxaldehyde ' ' I ' ' ' ■ I 31 15.40 15.60 15.80 16.00

60 88 5000

44 17 .....I , —H— T’16111T3T • i ’ * * * i ‘ 1as*s****.****1* m/z-> 10 20 30 40 50 60 70 80 90 100 110 120

5167.D HP022702.M Thu Mar 07 22:57:42 2002 Page 1

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