Volatile organic compounds blank results, Mar 8 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\02marll\5180D.D Vial: 8 Acq On : 11 Mar 2002 6:35 pm Operator: 201-wb Sample : nyc dup Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 3 1,3,5-Cycloheptatriene Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 18.58 0.03 ug/L 21920 CHLOROBENZENE-D5 21.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 4 2 Cyclobutene, 2-propenylidene- 92 C7H8 052097-85-5 2 3 Bicyclo[3.2.0]hepta-2,6-diene 92 C7H8 002422-86-8 2 4 Spiro[3.3]hepta-l,5-diene 92 C7H8 ______ 022635-78-5 2 Abundance Scan 857 (18.576 min): 5180D.D (-) m/z 91.00 100.00% 91 N

5000

18.20 18.40 18.60 18.80 _______________ 44____________________ 1’!0011011110—131033111—3311003121011 ______ ■ ■ i ■" ■ i1 ‘ —3378155012222211031333303333137771 m/z 92.10 70.84% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #970:1,3,5-Cycloheptatriene 91

5000 18.20 18.40 18.60 18.80 m/z 44.00 18.61% 65 27 38 A 51 । । •»■ ■ । > i»> > < i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #964: Cyclobutene, 2-propenylidene- 91

18.20 18.40 18.60 18.80 T 5000

65 77 51 npmmpmpmpmtpmtn I***IUNINLNt Hp n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #966: Bicyclo[3.2.O]hepta-2,6-diene 91

5000

39 66

m/z-> ..20....25 30.... l„.. 51 mpt .mgm 35 40 45 50 55 60 65 70 75 80 85 90 95 100 ‘•i■•■■i ■■

5180D.D HP022702.M Mon Mar 11 19:15:03 2002 Page 3

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