Volatile organic compounds results, Mar 7 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\02mar07\5164D.D Vial: 13 Acq On 7 Mar 2002 8:07 pm Operator: 201-wb Sample nyc dup Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxolan-2-one Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.73 0.03 ug/L 23244 1,4-DIFLUOROBENZENE 15.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dioxolan-2-one 88 C3H403 000096-49-1 4 2 Hydrazine, 1,2-diethyl- 88 C4H12N2 001615-80-1 4 3 1,2-Hydraz inedicarboxaldehyde 88 C2H4N2021 000628-36-4 4 4 3-Hexanone, 2-methyl- 114 C7H140 _______ 007379-12-6 4 Abundance Scan 691 (15.732 min): 5164D.D (-) m/z 114.05 100.00% 1’4

5000 63 88 15.40 15.60 15.80 16.00 ' 44 1 ■ ■ ■! ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ i 1 ' i ■ • ■ ■ i • ■ • ■ i ■' ■ ■ i ■ ■ ‘ p-r-n-p-n-rp-r- m/z 63.05 26.30% m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62892:1,3-Dioxolan-2-one 29

5000 43 -n-p-r-n-p- ‘ ' I ' ‘ ‘ ' I ' ' ' ‘ I 88 15.40 15.60 15.80 16.00 m/z 88.10 26.01% 58 H4 TImmPPTIT i ■1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #840: Hydrazine, 1,2-diethyl- 31 59 88 ■n-p-r-n-p TT-p-r-r-p-T-r-r-p 15.40 15.60 15:80 16.00 5000 m/z 43.95 13.40% 44 73 /ww/Mwi | i TI’ 11 “' I'1'1" I “ i • ■ ' ■ i ■ • ■ ‘ i ■ ■ ■ ■ i ‘1

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #781:1,2-Hydrazinedicarboxaldehyde 31 15.40 15.60 15.80 16.00

60 88 5000

44

/z--> 1 17 ■ 11 • ■ 11 ' ■ 10 20 '■'"I II'" I" 30 40 50 60 T-p-m-p-TT 70 80 90 i' ■ ■ ■ i ■1 ■ ■ i ■ ■ ■ ■ i ■1

100 110 120

5164D.D HP022702.M Thu Mar 07 20:47:08 2002 Page 1

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