Volatile organic compounds results, Mar 7 2002

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Data File C:\HPCHEM\l\DATA\02mar07\0307C10C.D Vial: 2 Acq On 8 Mar 2002 9:06 am Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 1-(Propenylthio)prop-l-ene Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.70 0.03 ug/L 23000 1,4-DIFLUOROBENZENE 15.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2! 006843-45-4 3 3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 2 4 2,4,5-Trioxoimidazolidine 114 C3H2N2031 000120-89-8 2 Abundance Scan 689 (15.698 min): 030701OC.D (-) m/z 114.05 100.00% 1 4

5000

63 88 15.40 15.60 15.80 16.00 50 1 - m/z 62.95 21.74% i ■ ■1 ■ i ■ ■1 ■ 11 ■ i ■ ■ • ■ i ■ ' ' ' i ' ' ' ' I ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2940:1-(Propenylthio)prop-1-ene 1 4 41 99

5000 15.40 15.60 15.80 16.00 m/z 88.10 20.64% 59 73 85 47 I , i • • ■ ■ i ■ TIE ''' i ' II7 ‘ I 1 ' ' ' I ' • • ■ । • 1 1 1 1 " I 11 ' FTTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64088:2,4-Imidazolidinedione, 3-methyl- 1 4

15.40 15.60 15.80 16.00 58 m/z 50.05 14.36% 5000

86

42 71 1****)**’1** • i ■ ■' ■ i ■ ■1 ‘ i ■ i ■ ■ ‘ ■ i ■ ■ • ■ i 1 ■ ‘ ‘ i ■ ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance 29 #64087:3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 58 .. .. A... 15.40 15.60 15.80 16.00

5000 114

... , 41 86 68 —B—nTUBTrn/n/1.n ‘ ' i ■ bd/B1/C m/z-> 20 30 40 50 60 70 80 90 100 110 120

0307C10C.D HP022702.M Fri Mar 08 09:46:2'8 2002 Page 1

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