Volatile organic compounds results, Mar 7 2002

NYC 9/11 Public Portal Document Library Search Coinpound Report Data File C:\HPCHEM\l\DATA\02mar07\5033.D Vial: 6 Acq On 8 Mar 2002 4:46 am Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 1,3-Dioxolan-2-one Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.71 0.03 ug/L 23965 1,4-DIFLUOROBENZENE 15.05 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dioxolan-2-one 88 C3H403 000096-49-1 3 2 Sulfide, allyl methyl 88 C4H8S 010152-76-8 3 3 1,2-Hydrazinedicarboxaldehyde 88 C2H4N202! 000628-36-4 3 4 Propanoic acid, 2-methyl- 88 C4H802 000079-31-2 3 Abundance Scan 690 (15.715 mln): 5033.D (-) m/z 114.05 100.00% 1 4

5000 63 88 15.40 15.60 15.80 16.00

m/z-> 44 ■ ■ i • ■ ■ ‘ i ■ ■ ■11 ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ ‘ ■ i ■ ■ • ■ i ■ 10 20 30 40 50 60 70 80 X 100 110 120 90 '' i ■ ■ ■ ■ i ‘ • ‘ i'' m/z 62.95 27.90%

Abundance #62893:1,3-Dioxolan-2-one 29

43 88 5000 ................. ................... 15.40 15.60 15.80 16.00 15 m/z 88.10 22.42% 58 _ PP Bagus —d i 1 73 ■11'''11 ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■

/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62927: Sulfide, allyl methyl 41 * * i * * । ■ • ■ । • i • ■ • * । 73 88 15.40 15.60 15.80 16.00 5000 m/z 43.95 8.34 MWWWWWA 61

m/z-> 1 ■ i ■ ■''i11'11111111 10 20 30 40 50 M 60 70 80 90 100 ' —mmomp 110 120 Abundance #781:1,2-Hydrazinedicarboxaldehyde 31 TTT 15.40 15.60 15.80 16.00

60 88 5000

44 17

rn/Z“> • ■ I •" • • I • • 10 20 -H 30 40 50 ■ I' • ■ ■ i ■ ■ ■ ■ i ■ ■ 60 70 80 11211’1’7*11-111113 90 100 110 120

5033.D HP022702.M Fri Mar 08 05:26:03 2002 Page 1

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